Journal
PHYSICAL REVIEW B
Volume 80, Issue 15, Pages -Publisher
AMER PHYSICAL SOC
DOI: 10.1103/PhysRevB.80.155446
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Long-range interface correlations in C/Au/C and Ag/Si3N4 layered films consisting of metal nanoparticles embedded in amorphous matrices are investigated by atomic force microscopy, high-angle annular dark-field scanning transmission electron microscopy, x-ray reflectivity, and grazing-incidence small-angle x-ray scattering (GISAXS). We demonstrate that the GISAXS intensity of such systems is modulated by waveguiding and correlated roughness effects, which involve the use of a dynamical scattering theory to analyze the experimental data and to distinguish between both effects. Direct imaging methods and GISAXS experiments combined with quantitative analysis within the distorted wave-Born approximation thus provide complementary information. While no roughness correlation is observed in the C/Au/C trilayers, the surface roughness of the Si3N4 capping layers in the Ag/Si3N4 bilayers replicate the topography of the Ag nanoparticles resulting in a partial correlation, which decreases as the Si3N4 thickness increases.
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