Journal
PHYSICAL CHEMISTRY CHEMICAL PHYSICS
Volume 15, Issue 24, Pages 9907-9913Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3cp50691f
Keywords
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Funding
- National Basic Research Program of China (973 Program) [2012CB933402, 2011CB935700]
- Natural Science Foundation of China [91027028, 51161120361, 21274074]
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We report an improved Hummers method for synthesizing graphene quantum dots (GQDs) by directly oxidizing and etching graphite powders. The yield of GQDs is as high as 63 +/- 7% (by weight, wt%), suggesting this technique is suitable for producing GQDs on a large scale. The GQDs are nanocrystals with lateral dimensions in the range of 2-4 nm and an average thickness of around 1.3 nm. The emission peaks of as-prepared GQDs can be tuned in the range of 440 to 510 nm by varying the reaction conditions. Their fluorescence quantum yields were tested to be around 1%, which could be further increased to about 3% by hydrothermal treatment. These GQDs have low cytotoxicity and excellent biocompatibility, indicating that they are promising for biological applications.
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