Journal
PHYSICAL CHEMISTRY CHEMICAL PHYSICS
Volume 12, Issue 21, Pages 5653-5659Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c004103n
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Funding
- Research Foundation-Flanders (FWO-Vlaanderen, Belgium)
- Belgian Government
- HASYLAB at DESY
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A confocal setup based on polycapillary half-lenses was used to demonstrate three-dimensional (3D) spatially resolved mu-XANES in fluorescence detection mode at the DUBBLE XAS station of the ESRF (BM26A). The incoming beam was focused using a polycapillary half-lens and a second glass polycapillary was placed in front of the energy dispersive detector to establish the confocal detection. The full-width-half-maxima along the main axes of the resulting ellipsoidal detection volume were 18.5 x 12.0 x 10.0 mu m(3) at the Cu K-edge. The confocal mu-XANES mode is applied in the 3D resolved study of mineral inclusions in rare natural diamonds at the Fe K edge.
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