Journal
ULTRAMICROSCOPY
Volume 148, Issue -, Pages 105-114Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.ultramic.2014.10.006
Keywords
Convergent-beam electron diffraction; Dynamical electron scattering; Artificial neural networks; Inverse problems; Three-dimensional characterization
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Funding
- Carl Zeiss Foundation
- German Research Foundation [KO 2911/7-1]
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For full three-dimensional information retrieval from transmission electron microscope data, retrieving the third-dimension (beam-direction) information is an important challenge. Recently, we have developed an artificial-neural-network-based retrieval algorithm suitable for retrieving three-dimensional nanoscale crystal parameters like strain, including with noisy data (R.S. Pennington, W. Van den Broek, C.T. Koch, Phys, Rev, B 89 (20) (2014) 205409 [12]). In this work, we examine how reciprocal-space sampling conditions influence the retrieved crystal parameters, using crystal tilt as an example parameter, and demonstrate retrieval for 2.5 nm depth resolution. For noise-free data, we find that the total reciprocal-space area is the key parameter; however, when the data are noisy, the number of reciprocal-space points and the amount of noise are also influential. We also apply our algorithm to a simulated bent specimen, and recover the bending as expected. Guidelines for experimental applications are also discussed. (C) 2014 Elsevier B.V. All rights reserved.
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