Journal
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS
Volume 189, Issue 2, Pages 285-292Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/10426507.2013.819868
Keywords
Sulfamides; amine-exchange reactions; microwave irradiation
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Funding
- Ondokuz Mayis University [F-286]
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Microwave-assisted synthesis of some substituted open-chain and cyclic sulfamides, by amine-exchange reaction, was studied in a modified domestic microwave oven. Reaction times and yields under microwave radiation were compared with classical heating. Synthesis of the sulfamides under microwave irradiation gave better yields with the desired compounds, and in considerably reduced reaction times, than those obtained by classical heating. [Supplementary materials are available for this article. Go to the publisher's online edition of Phosphorus, Sulfer, and Silicon and the Related Elements for the following free supplemental files: Additional figures.]
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