Journal
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS
Volume 185, Issue 11, Pages 2375-2381Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/10426501003664176
Keywords
Resin-bound acylhydrazine; solid phase synthesis; 1; 3; 4-thiadiazole
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Funding
- National Natural Science Foundation of China [20802068]
- Education Department of Zhejiang Province [20070015]
- Science and Technology Department of Zhejiang Province [2007C2116]
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A highly efficient, solid-phase synthesis of 2-arylamino-5-(4-hydroxy-phenyl)-1,3,4-thiadiazole derivatives under mild conditions has been developed. The 1,3,4-thiadiazole derivatives were synthesized from resin-bound acylhydrazines in several steps, which gave 78-88% overall yields and excellent purities of the products.
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