4.1 Article

An Approach to Disulfide Synthesis Promoted by Sulfonyl Chloride in Sodium Bicarbonate Aqueous Media

Journal

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS
Volume 184, Issue 10, Pages 2553-2559

Publisher

TAYLOR & FRANCIS LTD
DOI: 10.1080/10426500802529051

Keywords

Aqueous media; disulfides; sulfonyl chloride

Funding

  1. Natural Science Foundation of Zhejiang Province [Y4080107]
  2. Technology Program of Zhejiang Province [2003C31026, 2005C31036]

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A mild and efficient protocol for the synthesis of disulfides in aqueous media using mercaptans promoted by sulfonyl chloride is reported. This reaction offers the advantages of mild reaction conditions, short reaction time, high yields, and simple operation.

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