Journal
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS
Volume 184, Issue 4, Pages 846-856Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/10426500802715551
Keywords
CP cross-coupling reaction; phosphine-borane; vinylphosphine; vinyl tosylate
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Funding
- Ministere de la Recherche et des Nouvelles Technologies,
- CNRS (Centre National de la Recherche Scientifique)
- Region Basse-Normandie
- European Union (FEDER funding)
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Vinylphosphine-borane complexes are efficiently synthesized by palladium-catalyzed CP cross-coupling of vinyl tosylates with diphenylphosphine-borane. Both activated and unactivated vinyl tosylates are successfully used. The vinylphosphine derivatives are purified by chromatography on silica gel.
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