Journal
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS
Volume 183, Issue 5, Pages 1229-1235Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/10426500701613170
Keywords
2-mercaptoquinoline-3-carbaldehyde; phenoxyacetic acid; solvent free; thiopyrano[2,3-b]quinolin-2-one
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A series of some new thiopyrano[2,3-b]quinolin-2-one 2a-i have been synthesized by the one pot reaction between 2-mercaptoquinoline-3-carbaldehyde 1a-i and phenoxyacetic acid using TEA catalyst under microwave irradiation in solvent free conditions. The procedure is simple, environmentally benign and occurs in good yields. All the newly synthesized compounds were characterized by elemental analyses, IR, H-1 NMR and mass spectral data.
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