4.4 Article

Coupled motion of [10-10] tilt boundaries in magnesium bicrystals

Journal

PHILOSOPHICAL MAGAZINE
Volume 92, Issue 12, Pages 1499-1522

Publisher

TAYLOR & FRANCIS LTD
DOI: 10.1080/14786435.2011.648377

Keywords

magnesium alloys; creep testing; crystal growth; bicrystals; tilt boundaries; grain boundary motion

Funding

  1. General Motors/Brown University Collaborative Research Laboratory on Computational Materials Science

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Magnesium bicrystals were grown with symmetric and asymmetric tilt boundaries about the [10-10] axis using the vertical Bridgman technique. Isothermal constant load tensile tests were conducted on these bicrystals in the temperature range 300-500 degrees C and relative displacements of the two grains were measured to obtain an appreciation for grain boundary motion characteristics. Coupled grain boundary motion was noted in almost all cases with the degree of tangential motion versus migration changing with tilt misorientation, temperature and applied stress. Specifically, within the family of symmetric bicrystals evaluated, a minimum in grain boundary displacement in the specimen plane was observed at a tilt misorientation of 20 degrees. In specific stress/temperature regimes, rigid body sliding was observed for the particular case of a 35 degrees asymmetric tilt misorientation. The ease of basal and prism slip in magnesium at the temperatures considered and the consequential impingement of intragranular dislocations on the bicrystal boundary and their decomposition and motion along the boundary are thought to play an important role in the observed coupled motion of these tilt boundaries.

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