Journal
ORGANOMETALLICS
Volume 33, Issue 1, Pages 429-432Publisher
AMER CHEMICAL SOC
DOI: 10.1021/om401108b
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Funding
- U.S. National Science Foundation [CHE-0848248, CHE-1152123]
- University of Pennsylvania
- Division Of Chemistry
- Direct For Mathematical & Physical Scien [1413945] Funding Source: National Science Foundation
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The Tebbe reagent, [Cp2Ti(mu(2)-Cl)(mu(2)-CH2)AlMe2] (1), has finally been structurally characterized due to the fortuitous formation of cocrystals of 1 and [Cp2Ti(mu(2)-Cl)(2)AlMe2] (2). Single crystals of 1 and 2, despite being extremely reactive and forming an amorphous white coat, can be mounted and data collected to high resolution, thereby providing for the first time a solid-state representation of a titanium methylidene adduct with diphilic AlClMe2.
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