Journal
ORGANOMETALLICS
Volume 32, Issue 20, Pages 5887-5898Publisher
AMER CHEMICAL SOC
DOI: 10.1021/om400474e
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- Deutsche Forschungsgemeinschaft (DFG) through the Emmy-Noether program [WA 2513/2-1, WA 2513/2-2]
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Bulky pyrrolyl ligands have been used for the synthesis of diazaferrocenes, which have been characterized by various spectroscopic techniques, including X-ray diffraction for rac-[{eta(5)-2,3,5-(Me3C)(3)C4HN}(2)Fe]. Chemical oxidation of diazaferrocenes to the corresponding diazaferrocenium cations has been accomplished with AgSbF6. In addition, EPR and Mossbauer spectroscopic, electrochemical, and density function theory (DFT) studies have provided a more detailed understanding of the electronic structures of these complexes.
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