Journal
ORGANOMETALLICS
Volume 31, Issue 17, Pages 6312-6316Publisher
AMER CHEMICAL SOC
DOI: 10.1021/om300566m
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Funding
- MINECO [CTQ2011-24502, CSD2006-003]
- Junta de Andalucia [P07-FQM-02745]
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A novel bis-styrene IPrNi0 derivative has been synthesized from the reaction of Ni(COD)(2) and free 1,3-bis(2,6-diisopropylphenyl)imidazolidene (IPr) ligand in the presence of styrene. The complex has been characterized by spectroscopic data as well as by X-ray crystallography. Its catalytic performance in the amination reaction of aryl tosylates is also reported. The catalytic reactions proceed in a very selective manner, affording moderate to high yields of cross-coupling products in short reaction times at 110 degrees C.
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