Journal
ORGANOMETALLICS
Volume 31, Issue 21, Pages 7586-7590Publisher
AMER CHEMICAL SOC
DOI: 10.1021/om3008794
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- Deutsche Forschungsgemeinschaft (DFG)
- Alexander von Humboldt Stiftung
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Reaction of heteroleptic silylenes LSD( (L = PhC(NtBu)(2); X = PPh2 (1), NPh2 (2), NMe2 (3), OtBu (4)) with N2O resulted in the oxidized dimeric product [LSi(X)(mu-O)](2) (X = PPh2 (5), NPh2 (6), NMe2 (7), OtBu (8)), which contains a four -membered Si2O2 ring. Compounds 5-8 were characterized by spectroscopic and spectrometric techniques. The molecular structures of 5-8 were established by single-crystal X-ray structure analysis.
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