Journal
ORGANOMETALLICS
Volume 31, Issue 6, Pages 2124-2127Publisher
AMER CHEMICAL SOC
DOI: 10.1021/om300114e
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Funding
- National Natural Science Foundation of China [20872089, 21072129]
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Homocoupling and cross-coupling of electron-deficient arenes, including nitrobenzene, (trifluoromethyl)benzene, ethyl benzoate, etc., have been developed to afford biaryls using a catalytic system of Pd(OAc)(2)/trifluoroacetic acid (TFA)/O-2 or K2S2O8. The crucial step is to tune the concentrations of arenes and the loading of TFA carefully to enhance the reaction rates and the selectivity of these couplings involving dual C-H activation.
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