Journal
ORGANOMETALLICS
Volume 28, Issue 15, Pages 4252-4253Publisher
AMER CHEMICAL SOC
DOI: 10.1021/om900476g
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Reaction of Mes(2)BF with trimethylsilyl triflate (Me3SiOTf) and [Ag(IMe2][Ag2I3] (IMe = 1,3-dimethylimidazol-2-ylidene) in refluxing chlorobenzene affords the carbene-stabilized borenium salt [(IMe)BMes(2)]OTf ([I][OTf]). As indicated by cyclic voltammetry, [I](+) is reversibly reduced to produce a radical that has been characterized by EPR spectroscopy.
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