Journal
ORGANIC PROCESS RESEARCH & DEVELOPMENT
Volume 18, Issue 10, Pages 1181-1190Publisher
AMER CHEMICAL SOC
DOI: 10.1021/op500177w
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- Research Council of Norway
- University of Bergen
- GE Healthcare
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Acetylation of 1 with acetic anhydride, an important step in the preparation of iohexol, gave the corresponding acetanilide and minor amounts of a few byproducts, whose structures have been elucidated. Among the byproducts were some 1,3-oxazolidines which survived when the reaction was quenched by adding methanol and water under strong acidic conditions.
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