Journal
ORGANIC PROCESS RESEARCH & DEVELOPMENT
Volume 15, Issue 3, Pages 693-697Publisher
AMER CHEMICAL SOC
DOI: 10.1021/op2000223
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Funding
- Commonwealth Scholarship Commission
- Royal Society of Chemistry
- BP Endowment
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A general method for the continuous processing of suspensions and particulates is reported. A commercially available agitating cell reactor which uses a transverse mixing motion to maintain solids in suspension has been successfully applied to a salt-forming reaction. The flow device delivered 208 g of N-iodomorpholinium hydroiodide salt over a 9-h period (equating to 3.88 kg/week) under optimized conditions. The reactor is suitable for the medium-scale (5 kg) processing of solid-forming reactions and appears to offer the potential for a variety of more complex applications.
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