Journal
ORGANIC PROCESS RESEARCH & DEVELOPMENT
Volume 15, Issue 3, Pages 717-720Publisher
AMER CHEMICAL SOC
DOI: 10.1021/op200037n
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Funding
- National Science Foundation [CHE-0847262]
- University of Connecticut
- Division Of Chemistry
- Direct For Mathematical & Physical Scien [0847262] Funding Source: National Science Foundation
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Using a continuous-flow approach, it is possible to perform alkoxycarbonylation reactions of aryl iodides. Optimized reactor design allows for adequate mixing of gaseous and liquid reagents. Reactions are performed at rates of around 3 mL/min and at concentrations of 1 M, allowing for significant volumes to be processed per unit time. Palladium acetate (0.5 mol %) is used as the catalyst without the need for an additional ligand.
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