Journal
ORGANIC PROCESS RESEARCH & DEVELOPMENT
Volume 13, Issue 4, Pages 764-768Publisher
AMER CHEMICAL SOC
DOI: 10.1021/op9000725
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Funding
- National High Technology Research and Development Program of China [2007AA05Z454]
- Innovation Scientists and Technicians Troop Construction Projects of Henan Province [084200510015]
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Palladium-catalyzed cyanation of aryl halides is an often capricious reaction and lacks robustness due to catalyst poisoning by oxygen. In this report, an open-air and robust method for large-scale cyanation was developed and the use of commercially available i-propanol as an additive was critical for achieving the open-air, robust and scaleable process. Under the protection by i-propanol the catalyst life was significantly prolonged.
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