Journal
ORGANIC PROCESS RESEARCH & DEVELOPMENT
Volume 13, Issue 5, Pages 999-1002Publisher
AMER CHEMICAL SOC
DOI: 10.1021/op900129w
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The nitration of benzaldebyde can be carried out in a safe manner in continuous mode using a microreactor system. Choice of a micromixer was seen to affect the performance of this two-phase reaction significantly The reaction time could he brought down to 2 min by increasing the reaction temperature and thereby taking advantage of higher heat transfer area. The simple T-micromixer is seen to be inefficient for two-phase reactions. Further scope of process intensification is also discussed.
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