Journal
ORGANIC PROCESS RESEARCH & DEVELOPMENT
Volume 13, Issue 3, Pages 634-637Publisher
AMER CHEMICAL SOC
DOI: 10.1021/op800296d
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The ethoxycarbonylation of iodobenzene was performed on the 1 mol scale in batch mode using microwave heating. The reaction was performed using both an excess and a near stoichiometric loading of carbon monoxide, comparable yields being obtained. Six different alkoxycarbonylation reactions were then performed simultaneously on the 50 mmol scale using a near-stoichiometric loading of carbon monoxide with excellent conversions in each case.
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