Journal
ORGANIC PROCESS RESEARCH & DEVELOPMENT
Volume 12, Issue 6, Pages 1078-1088Publisher
AMER CHEMICAL SOC
DOI: 10.1021/op8001239
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Funding
- University of Connecticut Research Foundation
- American Chemical Society Petroleum Research Foundation [45433-AC1]
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A range of synthetic transformations have been scaled up successfully using a sealed-vessel multimode microwave unit. These include metal-catalyzed couplings, synthesis of heterocycles, reactions under an atmosphere of reactive gas and two-step one-pot procedures. Also, observations have been made along the way that are of use to chemists addressing scale-up of microwave-promoted reactions.
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