Journal
ORGANIC LETTERS
Volume 20, Issue 18, Pages 5956-5959Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.8b02669
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Funding
- Science and Engineering Research Board, DST [EMR/2014/000235]
- ISF-UGC Joint Research Program Framework [2253]
- UGC-New Delhi
- IIT Bombay
- DST
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The first total synthesis of the trisaccharide repeating unit of the O-specific polysaccharide of Pseudomonas fluorescens BIM B-582 is reported. This efficient synthesis involves consecutive 1,2-cis glyco-sylations including beta-L-rhamnosylation and alpha selective coupling of rare 4-deoxy-D-xylo-hexose as the key steps. The synthetic trisaccharide is equipped with an aminopropyl linker at the reducing end to allow for conjugation to proteins and microarrays for further immunological studies.
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