Journal
ORGANIC LETTERS
Volume 20, Issue 15, Pages 4401-4405Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.8b01524
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Funding
- JSPS KAKENHI [JP15KT0061, JP17H03971]
- AMED [J17am0101092j0001]
- Hoansha Foundation
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Gold(I)-catalyzed cascade cyclization of 1,4-diyn-3-ones with a pyridine N-oxide enabled direct construction of a benzo[6,7]cyclohepta[1,2-b]furan scaffold with the formation of four bonds. This reaction would proceed through oxidative cyclization, alkynyl migration, and 5-endo-dig type cyclization. Synthesis of benzotropone-fused naphtho[1,2-b]furans through a two-step sequence, including epoxidation and In(OTf)(3)-catalyzed intramolecular carbon carbon bond formation, is also presented.
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