Journal
ORGANIC LETTERS
Volume 16, Issue 18, Pages 4920-4923Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol502439m
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Funding
- JSPS [26810060]
- MEXT
- Special Project of Okayama University
- Grants-in-Aid for Scientific Research [26810060] Funding Source: KAKEN
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A direct selenation of inert C-H bonds of benzamide derivatives and their related compounds with diselenides has been achieved with the palladium catalyst. The reaction was compatible with a variety of functional groups, including a bromo group. Primitive mechanistic insights revealed that the reaction proceeded through a C H bond cleavage and the sequential oxidative addition of diselenides. The present synthetic method can be applied to the facile synthesis of selenoxanthone which can be regarded as promising heterocyclic materials.
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