Journal
ORGANIC LETTERS
Volume 15, Issue 2, Pages 406-409Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol3034059
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Funding
- National Science Foundation of China [21002045, 21272096]
- Fundamental Research Funds for the Central Universities [lzujbky-2012-55]
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A copper-catalyzed decarboxylative trifluoromethylation of various alpha,beta-unsaturated carboxylic acids by using a stable and inexpensive solid, sodium trifluoromethanesulfinate (CF3SO2Na, Langlois reagent), was developed. In addition, an Iron-catalyzed difluoromethylation of aryl-substituted acrylic acids by using zinc difluoromethanesulfinate (DFMS, (CF2HSO2)(2)Zn, Baran reagent) via a similar radical process was also achieved.
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