Journal
ORGANIC LETTERS
Volume 15, Issue 11, Pages 2620-2623Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol400801k
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Funding
- Agency for Science Technology and Research (A*STAR)
- National Research Foundation (NRF) of Singapore
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The cyclic cystine-knot peptide, kalata B1, was synthesized by employing a novel Fmoc-compatible thioethylalkylamido (TEA) thioester surrogate via an N-S acyl shift followed by a thiol-thioester exchange reaction. TEA thioester surrogate is cost-effective, conveniently prepared in one-step with starting materials, readily available from commercial sources, and highly efficient in preparing peptide thioesters.
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