Journal
ORGANIC LETTERS
Volume 15, Issue 4, Pages 968-971Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol4002015
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Funding
- NSFC [21125206, 21021001]
- National Basic Research Program of China (973 Program) [2010CB833300]
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An asymmetric exo-Diels-Alder reaction of alpha-methylene carbonyl compounds, generated In situ from stable methiodide salts of Mannich bases, with 2,4-dienals, has been developed through trienamine activation of a chiral secondary amine. A spectrum of spirocyclanes with high molecular complexity was efficiently constructed In moderate to excellent diastereo- and enantioselectivity.
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