Journal
ORGANIC LETTERS
Volume 15, Issue 11, Pages 2574-2577Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol400877q
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Funding
- Chinese Academy of Sciences
- Ministry of Education [SRFDP 20123402110040]
- National Science Foundation of China [21102138]
- University of Science and Technology of China (USTC)
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A practical Pd(II)/Pd(IV)-catalyzed carboxyl-directed C-H activation/C-O cyclization to construct biaryl lactones has been developed. The synthetic utility of this new reaction was demonstrated in an atom-economical and operationally convenient total synthesis of the natural product cannabinol from commercially available starting materials, with the newly developed method used for two key steps.
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