Journal
ORGANIC LETTERS
Volume 15, Issue 3, Pages 504-507Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol303310u
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- Science Foundation Ireland [09/RFP/CHS2256]
- Science Foundation Ireland (SFI) [09/RFP/CHS2256] Funding Source: Science Foundation Ireland (SFI)
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The use of intramolecular thiyl radical cyclizations for the synthesis of thiosugars has been investigated, and a new free-radical-based methodology for the synthesis of biologically important thiosugars has been developed. The methodology is mild and proceeds via either 6-endo or 5-exo cyclization to furnish the thiosugar ring. This represents the first examples of thiyl radical cyclizatlon being applied to the synthesis of thiosugars.
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