Journal
ORGANIC LETTERS
Volume 15, Issue 9, Pages 2314-2317Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol401004r
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Funding
- University of Delaware (UD)
- ACS Petroleum Research Fund [51706-DNI1]
- NSF
- NIH [NSF MIR CHE0421224, CHE1229234, NSF CRIF MU CHE0840401, NIH P20 GM103541, NIH S10 RR02692]
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [1229234] Funding Source: National Science Foundation
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For the first time, a general catalytic procedure for the cross-coupling of primary amides and alkylboronic acids is demonstrated. The key to the success of this reaction was the identification of a mild base (NaOSiMe3) and oxidant (di-tert-butyl peroxide) to promote the copper-catalyzed reaction in high yield. This transformation provides a facile, high-yielding method for the monoallrylation of amides.
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