Journal
ORGANIC LETTERS
Volume 15, Issue 6, Pages 1346-1349Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol400289v
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Funding
- EPSRC
- European Research Council (ERC) [246785]
- EPSRC [EP/E052185/1, EP/I038071/1, EP/K03927X/1] Funding Source: UKRI
- Engineering and Physical Sciences Research Council [EP/I038071/1, EP/K03927X/1, EP/E052185/1] Funding Source: researchfish
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The synthesis of highly enantioenriched alpha-heterocyclic tertiary alcohols has been achieved via lithiation-borylation of a configurationally stable lithiated carbamate and heterocyclic pinacol boronic esters followed by oxidation. Protodeboronation of the alpha-heterocyclic tertiary boronic esters using TBAF center dot 3H(2)O or CsF gave highly enantioenriched 1-pyridyl-1-arylethanes in high er.
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