Journal
ORGANIC LETTERS
Volume 15, Issue 23, Pages 5978-5981Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol401273k
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Funding
- Project PROCIP [ANR-2010-CD2I-013-01]
- program Eramus Mundus
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A safe, straightforward, and atom economic approach for the oxidation of aliphatic aldehydes to the corresponding carboxylic acids within a continuous flow reactor is reported. Typically, the reaction is performed at room temperature using 5 bar of oxygen in PFA tubing and does require neither additional catalysts nor radical initiators except for those already contained in the starting materials. In some cases, a catalytic amount of a Mn(II) catalyst is added. Such a flow process may prove to be a valuable alternative to traditionally catalyzed aerobic processes.
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