Journal
ORGANIC LETTERS
Volume 15, Issue 4, Pages 752-755Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol3026445
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Funding
- National Research Foundation of Korea
- Korean Government (MEST) [NRF-2012-1012596]
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The palladium-catalyzed diacetoxylation and trifluoromethanesulfonic acid-catalyzed diacetoxylation using inexpensive and environmentally friendly hydrogen peroxide and peracetic acid were successfully conducted with the help of microchemical technology. Excellent yield and selectivity were achieved in significantly shortened reaction times without the decomposition of explosive oxidants and further transformation of unstable products, offering a safe and efficient alternative to traditional methods for alkene diacetoxylation.
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