Journal
ORGANIC LETTERS
Volume 15, Issue 6, Pages 1306-1309Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol4002448
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Funding
- Ministry of Education, Culture, Sports, Science and Technology (MEXT) of Japan [12045232]
- Grants-in-Aid for Scientific Research [24105530, 23390007, 24102525, 12045232] Funding Source: KAKEN
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Chemoselective hydrogenation of unsaturated compounds bearing an o-nitrobenzenesulfonyl (Ns)-amide moiety, affording the corresponding saturated compounds, was accomplished efficiently without loss of the nitro group by using the Pd/MS3A catalyst and a H-2 balloon. Partial hydrogenation of alkynes bearing an Ns group to corresponding cis alkenes was achieved with the combination of the Pd/BN catalyst and an additive (diethylenetriamine or acetic acid).
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