Journal
ORGANIC LETTERS
Volume 14, Issue 6, Pages 1620-1623Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol3003755
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- Japanese Ministry of Education, Culture, Sports, Science and Technology
- Japan Society for the Promotion of Science
- Grants-in-Aid for Scientific Research [21106005, 21106001, 23350017] Funding Source: KAKEN
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A novel asymmetric formal [3 + 2] cycloaddition reaction for the synthesis of 1,3-dioxolanes using cinchona-alkaloid-thiourea-based bifunctional organocatalysts is reported. The reaction proceeds via the formation of hemiacetal intermediates between gamma-hydroxy-alpha,beta-unsaturated ketones and aldehydes.
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