Journal
ORGANIC LETTERS
Volume 14, Issue 13, Pages 3412-3415Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol301386k
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- ARC
- Monash Research Accelerator Program
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A range of spirocyclic gamma-lactones have been prepared exploiting a Beckwith-Dowd ring expansion cascade involving 1-, 3-, 4-, and 5-carbon expansion of cyclopentanone and cyclohexanone followed by 5-exo-trig or 5-exo-dig cyclization. This radical cascade reaction can be achieved with various substrates to provide a broad range of gamma-lactones spirofused to 6- to 10-membered cycloalkanones.
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