Journal
ORGANIC LETTERS
Volume 14, Issue 23, Pages 5932-5935Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol302848m
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Funding
- National Institute of General Medical Sciences [R01 GM084927]
- National Science Foundation
- Vietnam Education Foundation
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Aerobic hydroperoxidation of Meldrum's acid derivatives via a Cu(II)-catalyzed process is presented. The mild reaction conditions are tolerant to pendant unsaturation allowing the formation of endoperoxides via electrophilic activation. Cleavage of the O-O bond provides 1,n-diols with differentiation of the hydroxy groups.
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