Journal
ORGANIC LETTERS
Volume 14, Issue 6, Pages 1632-1635Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol300390k
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Funding
- Japan Society for the Promotion of Science (JSPS) [20002004, 22590002]
- Research Foundation for Pharmaceutical Sciences
- Mochida Memorial Foundation for Medical and Pharmaceutical Research
- Uehara Memorial Foundation
- Grants-in-Aid for Scientific Research [10J01765, 20002004] Funding Source: KAKEN
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A novel synthetic route to (-)-anisatin has been developed. Our synthesis features a rhodium-catalyzed 1,4-addition of an arylboronic acid, an intramolecular Diels Alder reaction of an ortho-quinone monoketal, a stereoselective [2,3]-Wittig rearrangement, and construction of the oxabicyclo [3.3.1] skeleton via cleavage of an epoxide by a primary amide.
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