Journal
ORGANIC LETTERS
Volume 15, Issue 2, Pages 410-413Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol3034093
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Funding
- National Natural Science Foundation of China [20562012, 21162033, 21062029]
- Natural Science Foundation of Yunnan Province [2009CD007]
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The title compound was synthesized mainly by palladium catalytic coupling, cyclopropyl ring-opening rearrangement, epoxidation, Swern oxidation, demethanol reactions, and selective reduction. This synthesis was achieved in 16 steps with 9.7% overall yield. Unfortunately, the published spectroscopic data do not match with those of our synthetic compound.
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