Journal
ORGANIC LETTERS
Volume 14, Issue 19, Pages 5154-5157Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol302498v
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A highly convergent total synthesis of 7',8'-dihydroaigialospirol is described. Key steps of the synthesis include a Nozaki-Hiyama-Kishi (NHK) coupling of an iodoalkyne with an advanced phthalide-aldehyde and a remarkable one-pot acid-mediated global deprotection/spiroacetalization.
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