Journal
ORGANIC LETTERS
Volume 14, Issue 7, Pages 1880-1883Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol300476f
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Funding
- National Institutes of Health [GM038436]
- Eli Lilly
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A concise, enantioselective synthesis of (+)-crocacin C is described, featuring a highly diastereoselective mismatched double asymmetric delta-stannylcrotylboration of the stereochemically demanding chiral aldehyde 9 with the bifunctional crotylborane reagent (S)-E-10. The total synthesis of (+)-crocacin C was accomplished in seven steps (longest linear sequence) starting from commercially available precursors.
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