Journal
ORGANIC LETTERS
Volume 13, Issue 5, Pages 1086-1088Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol103128x
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Funding
- JSPS
- MEXT [1301]
- Grants-in-Aid for Scientific Research [21750086, 21350020] Funding Source: KAKEN
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Carboxylation of alkylboron compounds (alkyl-9-BBN) with CO2 proceeded in the presence of catalytic amounts of CuOAc/1,10-phenanthroline and a stoichiometric amount of (KOBu)-Bu-t. The alkylboranes are easily and widely available through the alkene hydroboration, and thus the overall process represents a reductive carboxylation of alkenes with CO2. The broad functional group compatibility and the inexpensiveness of the Cu/1,10-phenathoroline catalyst system are attractive features of this protocol.
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