Journal
ORGANIC LETTERS
Volume 13, Issue 3, Pages 510-513Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol102884g
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Funding
- DGI of Spain [CTQ2007-61048/BQU]
- Consejeria de Educacion y Ciencia of Principado de Asturias [IB08-088]
- FICYT of the Principado de Asturias
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Aryl nonaflates are employed as electrophiles in the Pd-catalyzed cross-coupling with tosylhydrazones affording di-, tri-, and tetrasubstituted olefins. Fine tunning of the reaction conditions are required to accomplish the coupling successfully, including the addition of LICI and the presence of small amounts of water. Under the optimized conditions, the reactions proceed with high yield and also high stereoselectivity depending on the nature of the coupling partners.
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