Journal
ORGANIC LETTERS
Volume 13, Issue 18, Pages 4946-4949Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol202049v
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Funding
- EPSRC
- EPSRC [EP/G007519/1] Funding Source: UKRI
- Engineering and Physical Sciences Research Council [EP/G007519/1] Funding Source: researchfish
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Arynes, generated from trimethylsilyl phenyltriflate precursors, have been found to react with thioureas via a formal pi-insertion into the C=S bond. The reaction contrasts with that of ureas, which proceeds via benzyne sigma-insertion into the C-N bond, and represents a new, operationally simple route to functionalized amidines.
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