Journal
ORGANIC LETTERS
Volume 13, Issue 14, Pages 3762-3765Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol201458q
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- Council of Scientific and Industrial Research (CSIR)
- Department of Science and Technology (DST), New Delhi
- Grants Commission (UGC), New Delhi
- CSIR, New Delhi
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A highly efficient one-pot three-component regioselective synthesis of 4-aryl-3-aroyl-2-methylsulfanyl-4,6,7,8-tetrahydrothiochromen-5-ones has been developed by annulation of beta-oxodithioesters with aldehydes and cyclic 1,3-diketones under solvent-free conditions promoted by P2O5. No cocatalyst or activator is needed in this protocol. The merit of this process is highlighted by its high efficiency of producing three new bonds and a stereocenter In one operation.
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