Journal
ORGANIC LETTERS
Volume 13, Issue 13, Pages 3312-3315Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol2010006
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Funding
- Cambridge European Trust
- EPSRC
- Royal Society
- EPSRC [EP/F069685/1] Funding Source: UKRI
- Engineering and Physical Sciences Research Council [EP/F069685/1] Funding Source: researchfish
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A new machine for conducting continuous flow processes at low temperatures on a laboratory scale is reported. The use of this cryogenic flow reactor has been demonstrated by the preparation of a variety of (hetero)aromatic boronic acids and esters via lithium halogen exchange chemistry. Furthermore, scale-up of the reaction conditions not only demonstrates the application of this device for the preparation of useful building blocks but also combines the ability to process n-butyllithium directly through pump heads attached to the unit.
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