Journal
ORGANIC LETTERS
Volume 13, Issue 11, Pages 2814-2817Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol200726v
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Funding
- Tufts University
- GAANN
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [0821508] Funding Source: National Science Foundation
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Dehydrative glycosylation reactions using 2-deoxy- and 2,6-dideoxy-sugar donors promoted by a combination of 3,3-dichloro-1,2-diphenylcyclopropene and tetrabutylammonium iodide (TBAI) are described. The reactions are a-selective and proceed under mild conditions at room temperature without the need for special dehydrating agents. The reaction is shown to be effective with a number of glycosyl acceptors, including those possessing acid and base sensitive functionality.
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