Journal
ORGANIC LETTERS
Volume 13, Issue 24, Pages 6414-6417Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol2027015
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- Novartis-MIT Center for Continuous Manufacturing
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Inter- and intramolecular ene-yne coupling reactions catalyzed by a species generated in situ via photolysis of CpRu(eta(6)-C6H6)PF6-an inexpensive, readily available, and shelf-stable complex-have been demonstrated under conditions of continuous flow. Importantly, the catalyst can be recovered quantitatively at the end of the reaction. Various functional groups are tolerated by the reaction, which affords skipped diene products in high yields.
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